Abstract

A one-step method for synthesizing nano-diamonds (NDs), femtosecond pulsed laser ablation, of bulk diamond in DI water is reported. The mean size of NDs is 3.0 nm observed by TEM. UV-Vis absorption spectrum reveals that there are two absorption peaks in NDs. For prepared NDs, it can be seen from emission spectrum that dual emission occurs under the excitation of either 260 nm or 280 nm, while the dual emission disappears after surface passivation. Moreover, the intensity of visible blue fluorescence emitted by NDs is significantly enhanced for passivated NDs. In addition, it is found that the ablation efficiency enhances with the increase of ablation power, which can be also verified by the intensity changing of UV-Vis absorption spectra. The maximum yield can reach to 8.2 mg·h−1 under 828 mW. These NDs emit stable blue emission and are synthesized by a rather simple green way, of which the NDs yield can meet the requirement of practical applications in terms of drug and gene delivery.

© 2019 Optical Society of America under the terms of the OSA Open Access Publishing Agreement

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  8. D. Li, X. Chen, Y. Gong, B. Zhang, Y. Liu, P. Jin, and H. Li, “Synthesis and Vacuum Cold Spray Deposition of Biofunctionalized Nanodiamond/Hydroxyapatite Nanocomposite for Biomedical Applications,” Adv. Eng. Mater. 19(12), 1700363 (2017).
    [Crossref]
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    [Crossref]
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    [Crossref]
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    [Crossref]
  28. S. L. Hu, F. Tian, P. K. Bai, S. R. Cao, J. Sun, and J. Yang, “Synthesis and luminescence of nanodiamonds from carbon black,” Mater. Sci. Eng., B 157(1-3), 11–14 (2009).
    [Crossref]
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    [Crossref]
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    [Crossref]
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    [Crossref]
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    [Crossref]
  36. K. B. Holt, “Undoped diamond nanoparticles: origins of surface redox chemistry,” Phys. Chem. Chem. Phys. 12(9), 2048–2058 (2010).
    [Crossref]
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    [Crossref]
  38. J. Robertson, “Electronic and atomic structure of diamond-like carbon,” Semicond. Sci. Technol. 18(3), S12–S19 (2003).
    [Crossref]
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    [Crossref]
  40. G. Xin, Y. Meng, Y. Ma, D. Ho, N. Kim, S. M. Cho, and H. Chae, “Tunable photoluminescence of graphene oxide from near-ultraviolet to blue,” Mater. Lett. 74, 71–73 (2012).
    [Crossref]
  41. C. T. Chien, S. S. Li, W. J. Lai, Y. C. Yeh, H. A. Chen, I. S. Chen, L. C. Chen, K. H. Chen, T. Nemoto, S. Isoda, M. W. Chen, T. Fujita, G. Eda, H. Yamaguchi, M. Chhowalla, and C. W. Chen, “Tunable Photoluminescence from Graphene Oxide,” Angew. Chem., Int. Ed. 51(27), 6662–6666 (2012).
    [Crossref]

2019 (3)

A. V. Shvidchenko, E. D. Eidelman, A. Y. Vul, N. M. Kuznetsov, D. Y. Stolyarova, S. I. Belousov, and S. N. Chvalun, “Colloids of detonation nanodiamond particles for advanced applications,” Adv. Colloid Interface Sci. 268, 64–81 (2019).
[Crossref]

C. Doñate-Buendía, M. Fernández-Alonso, J. Lancis, and G. Mínguez-Vega, “Overcoming the barrier of nanoparticle production by femtosecond laser ablation in liquids using simultaneous spatial and temporal focusing,” Photonics Res. 7(11), 1249 (2019).
[Crossref]

M. Gautam and D. Santhiya, “Pectin/PEG food grade hydrogel blend for the targeted oral co-delivery of nutrients,” Colloids Surf., A 577, 637–644 (2019).
[Crossref]

2018 (6)

R. Ye, X. Han, D. V. Kosynkin, Y. Li, C. Zhang, B. Jiang, A. A. Marti, and J. M. Tour, “Laser-Induced Conversion of Teflon into Fluorinated Nanodiamonds or Fluorinated Graphene,” ACS Nano 12(2), 1083–1088 (2018).
[Crossref]

L. Jiang, A. D. Wang, B. Li, T. H. Cui, and Y. F. Lu, “Electrons dynamics control by shaping femtosecond laser pulses in micro/nanofabrication: modeling, method, measurement and application,” Light: Sci. Appl. 7(2), 17134 (2018).
[Crossref]

L. Basso, F. Gorrini, N. Bazzanella, M. Cazzanelli, C. Dorigoni, A. Bifone, and A. Miotello, “The modeling and synthesis of nanodiamonds by laser ablation of graphite and diamond-like carbon in liquid-confined ambient,” Appl. Phys. A: Mater. Sci. Process. 124(1), 72 (2018).
[Crossref]

L.-S. Fan, L. Constantin, D.-W. Li, L. Liu, K. Keramatnejad, C. Azina, X. Huang, H. R. Golgir, Y. Lu, Z. Ahmadi, F. Wang, J. Shield, B. Cui, J.-F. Silvain, and Y.-F. Lu, “Ultraviolet laser photolysis of hydrocarbons for nondiamond carbon suppression in chemical vapor deposition of diamond films,” Light: Sci. Appl. 7(4), 17177 (2018).
[Crossref]

X. Bao, Y. Yuan, J. Chen, B. Zhang, D. Li, D. Zhou, P. Jing, G. Xu, Y. Wang, K. Hola, D. Shen, C. Wu, L. Song, C. Liu, R. Zboril, and S. Qu, “In vivo theranostics with near-infrared-emitting carbon dots-highly efficient photothermal therapy based on passive targeting after intravenous administration,” Light: Sci. Appl. 7(1), 91 (2018).
[Crossref]

Z. Cui, Y. Zhang, K. Xia, Q. Yan, H. Kong, J. Zhang, X. Zuo, J. Shi, L. Wang, Y. Zhu, and C. Fan, “Nanodiamond autophagy inhibitor allosterically improves the arsenical-based therapy of solid tumors,” Nat. Commun. 9(1), 4347 (2018).
[Crossref]

2017 (6)

D. Li, X. Chen, Y. Gong, B. Zhang, Y. Liu, P. Jin, and H. Li, “Synthesis and Vacuum Cold Spray Deposition of Biofunctionalized Nanodiamond/Hydroxyapatite Nanocomposite for Biomedical Applications,” Adv. Eng. Mater. 19(12), 1700363 (2017).
[Crossref]

X. B. Cheng, M. Q. Zhao, C. Chen, A. Pentecost, K. Maleski, T. Mathis, X. Q. Zhang, Q. Zhang, J. Jiang, and Y. Gogotsi, “Nanodiamonds suppress the growth of lithium dendrites,” Nat. Commun. 8(1), 336 (2017).
[Crossref]

L. Reinert, S. Suarez, T. Müller, and F. Mücklich, “Carbon Nanoparticle-Reinforced Metal Matrix Composites: Microstructural Tailoring and Predictive Modeling ,” Adv. Eng. Mater. 19(5), 1600750 (2017).
[Crossref]

D. Wang, X.-B. Li, D. Han, W. Q. Tian, and H.-B. Sun, “Engineering two-dimensional electronics by semiconductor defects,” Nano Today 16, 30–45 (2017).
[Crossref]

K. Turcheniuk and V. N. Mochalin, “Biomedical applications of nanodiamond (Review),” Nanotechnology 28(25), 252001 (2017).
[Crossref]

D. Zhang, B. Gokce, and S. Barcikowski, “Laser Synthesis and Processing of Colloids: Fundamentals and Applications,” Chem. Rev. 117(5), 3990–4103 (2017).
[Crossref]

2016 (3)

M. I. Setyawati, V. N. Mochalin, and D. T. Leong, “Tuning Endothelial Permeability with Functionalized Nanodiamonds,” ACS Nano 10(1), 1170–1181 (2016).
[Crossref]

H.-B. Jiang, Y.-L. Zhang, Y. Liu, X.-Y. Fu, Y.-F. Li, Y.-Q. Liu, C.-H. Li, and H.-B. Sun, “Bioinspired few-layer graphene prepared by chemical vapor deposition on femtosecond laser-structured Cu foil,” Laser Photonics Rev. 10(3), 441–450 (2016).
[Crossref]

R. Streubel, S. Barcikowski, and B. Gokce, “Continuous multigram nanoparticle synthesis by high-power, high-repetition-rate ultrafast laser ablation in liquids,” Opt. Lett. 41(7), 1486 (2016).
[Crossref]

2015 (1)

J. Xiao, P. Liu, and G. W. Yang, “Nanodiamonds from coal under ambient conditions,” Nanoscale 7(14), 6114–6125 (2015).
[Crossref]

2013 (1)

D. Z. Tan, S. F. Zhou, B. B. Xu, P. Chen, Y. Shimotsuma, K. Miura, and J. R. Qiu, “Simple synthesis of ultra-small nanodiamonds with tunable size and photoluminescence,” Carbon 62, 374–381 (2013).
[Crossref]

2012 (3)

V. N. Mochalin, O. Shenderova, D. Ho, and Y. Gogotsi, “The properties and applications of nanodiamonds,” Nat. Nanotechnol. 7(1), 11–23 (2012).
[Crossref]

G. Xin, Y. Meng, Y. Ma, D. Ho, N. Kim, S. M. Cho, and H. Chae, “Tunable photoluminescence of graphene oxide from near-ultraviolet to blue,” Mater. Lett. 74, 71–73 (2012).
[Crossref]

C. T. Chien, S. S. Li, W. J. Lai, Y. C. Yeh, H. A. Chen, I. S. Chen, L. C. Chen, K. H. Chen, T. Nemoto, S. Isoda, M. W. Chen, T. Fujita, G. Eda, H. Yamaguchi, M. Chhowalla, and C. W. Chen, “Tunable Photoluminescence from Graphene Oxide,” Angew. Chem., Int. Ed. 51(27), 6662–6666 (2012).
[Crossref]

2010 (3)

K. B. Holt, “Undoped diamond nanoparticles: origins of surface redox chemistry,” Phys. Chem. Chem. Phys. 12(9), 2048–2058 (2010).
[Crossref]

G. Eda, Y. Y. Lin, C. Mattevi, H. Yamaguchi, H. A. Chen, I. S. Chen, C. W. Chen, and M. Chhowalla, “Blue Photoluminescence from Chemically Derived Graphene Oxide,” Adv. Mater. 22(4), 505–509 (2010).
[Crossref]

N. G. Semaltianos, “Nanoparticles by Laser Ablation,” Crit. Rev. Solid State Mater. Sci. 35(2), 105–124 (2010).
[Crossref]

2009 (6)

D. Amans, A. C. Chenus, G. Ledoux, C. Dujardin, C. Reynaud, O. Sublemontier, K. Masenelli-Varlot, and O. Guillois, “Nanodiamond synthesis by pulsed laser ablation in liquids,” Diamond Relat. Mater. 18(2-3), 177–180 (2009).
[Crossref]

S. L. Hu, F. Tian, P. K. Bai, S. R. Cao, J. Sun, and J. Yang, “Synthesis and luminescence of nanodiamonds from carbon black,” Mater. Sci. Eng., B 157(1-3), 11–14 (2009).
[Crossref]

S. Osswald, V. N. Mochalin, M. Havel, G. Yushin, and Y. Gogotsi, “Phonon confinement effects in the Raman spectrum of nanodiamond,” Phys. Rev. B 80(7), 075419 (2009).
[Crossref]

A. Kromka, B. Rezek, M. Kalbacova, V. Baresova, J. Zemek, C. Konak, and M. Vanecek, “Diamond Seeding and Growth of Hierarchically Structured Films for Tissue Engineering,” Adv. Eng. Mater. 11(7), B71–B76 (2009).
[Crossref]

V. N. Mochalin and Y. Gogotsi, “Wet Chemistry Route to Hydrophobic Blue Fluorescent Nanodiamond,” J. Am. Chem. Soc. 131(13), 4594–4595 (2009).
[Crossref]

J. P. Boudou, P. A. Curmi, F. Jelezko, J. Wrachtrup, P. Aubert, M. Sennour, G. Balasubramanian, R. Reuter, A. Thorel, and E. Gaffet, “High yield fabrication of fluorescent nanodiamonds,” Nanotechnology 20(23), 235602 (2009).
[Crossref]

2008 (1)

Y. R. Chang, H. Y. Lee, K. Chen, C. C. Chang, D. S. Tsai, C. C. Fu, T. S. Lim, Y. K. Tzeng, C. Y. Fang, C. C. Han, H. C. Chang, and W. Fann, “Mass production and dynamic imaging of fluorescent nanodiamonds,” Nat. Nanotechnol. 3(5), 284–288 (2008).
[Crossref]

2007 (1)

G. W. Yang, “Laser ablation in liquids: Applications in the synthesis of nanocrystals,” Prog. Mater. Sci. 52(4), 648–698 (2007).
[Crossref]

2006 (1)

S. Osswald, G. Yushin, V. Mochalin, S. O. Kucheyev, and Y. Gogotsi, “Control of sp2/sp3 carbon ratio and surface chemistry of nanodiamond powders by selective oxidation in air,” J. Am. Chem. Soc. 128(35), 11635–11642 (2006).
[Crossref]

2005 (1)

C. X. Wang, Y. H. Yang, and G. W. Yang, “Thermodynamical predictions of nanodiamonds synthesized by pulsed-laser ablation in liquid,” J. Appl. Phys. 97(6), 066104 (2005).
[Crossref]

2004 (1)

É. M. Galimov, A. M. Kudin, V. N. Skorobogatskii, V. G. Plotnichenko, O. L. Bondarev, B. G. Zarubin, V. V. Strazdovskii, A. S. Aronin, A. V. Fisenko, I. V. Bykov, and A. Y. Barinov, “Experimental Corroboration of the Synthesis of Diamond in the Cavitation Process,” Dokl. Phys. 49(3), 150–153 (2004).
[Crossref]

2003 (1)

J. Robertson, “Electronic and atomic structure of diamond-like carbon,” Semicond. Sci. Technol. 18(3), S12–S19 (2003).
[Crossref]

2002 (1)

J. Robertson, “Diamond-like amorphous carbon,” Mater. Sci. Eng., R 37(4-6), 129–281 (2002).
[Crossref]

2001 (1)

T. L. Daulton, M. A. Kirk, R. S. Lewis, and L. E. Rehn, “Production of nanodiamonds by high-energy ion irradiation of graphite at room temperature,” Nucl. Instrum. Methods Phys. Res., Sect. B 175-177, 12–20 (2001).
[Crossref]

1993 (1)

S. Han, S. G. Prussin, J. W. Ager, L. S. Pan, D. R. Kania, S. M. Lane, and R. S. Wagner, “Radiation-Damage Study of Polycrystalline Cvd and Natural Type-Iia Diamonds Using Raman and Photoluminescence Spectroscopies,” Nucl. Instrum. Methods Phys. Res., Sect. B 80-81(1), 1446–1450 (1993).
[Crossref]

Ager, J. W.

S. Han, S. G. Prussin, J. W. Ager, L. S. Pan, D. R. Kania, S. M. Lane, and R. S. Wagner, “Radiation-Damage Study of Polycrystalline Cvd and Natural Type-Iia Diamonds Using Raman and Photoluminescence Spectroscopies,” Nucl. Instrum. Methods Phys. Res., Sect. B 80-81(1), 1446–1450 (1993).
[Crossref]

Ahmadi, Z.

L.-S. Fan, L. Constantin, D.-W. Li, L. Liu, K. Keramatnejad, C. Azina, X. Huang, H. R. Golgir, Y. Lu, Z. Ahmadi, F. Wang, J. Shield, B. Cui, J.-F. Silvain, and Y.-F. Lu, “Ultraviolet laser photolysis of hydrocarbons for nondiamond carbon suppression in chemical vapor deposition of diamond films,” Light: Sci. Appl. 7(4), 17177 (2018).
[Crossref]

Amans, D.

D. Amans, A. C. Chenus, G. Ledoux, C. Dujardin, C. Reynaud, O. Sublemontier, K. Masenelli-Varlot, and O. Guillois, “Nanodiamond synthesis by pulsed laser ablation in liquids,” Diamond Relat. Mater. 18(2-3), 177–180 (2009).
[Crossref]

Aronin, A. S.

É. M. Galimov, A. M. Kudin, V. N. Skorobogatskii, V. G. Plotnichenko, O. L. Bondarev, B. G. Zarubin, V. V. Strazdovskii, A. S. Aronin, A. V. Fisenko, I. V. Bykov, and A. Y. Barinov, “Experimental Corroboration of the Synthesis of Diamond in the Cavitation Process,” Dokl. Phys. 49(3), 150–153 (2004).
[Crossref]

Aubert, P.

J. P. Boudou, P. A. Curmi, F. Jelezko, J. Wrachtrup, P. Aubert, M. Sennour, G. Balasubramanian, R. Reuter, A. Thorel, and E. Gaffet, “High yield fabrication of fluorescent nanodiamonds,” Nanotechnology 20(23), 235602 (2009).
[Crossref]

Azina, C.

L.-S. Fan, L. Constantin, D.-W. Li, L. Liu, K. Keramatnejad, C. Azina, X. Huang, H. R. Golgir, Y. Lu, Z. Ahmadi, F. Wang, J. Shield, B. Cui, J.-F. Silvain, and Y.-F. Lu, “Ultraviolet laser photolysis of hydrocarbons for nondiamond carbon suppression in chemical vapor deposition of diamond films,” Light: Sci. Appl. 7(4), 17177 (2018).
[Crossref]

Bai, P. K.

S. L. Hu, F. Tian, P. K. Bai, S. R. Cao, J. Sun, and J. Yang, “Synthesis and luminescence of nanodiamonds from carbon black,” Mater. Sci. Eng., B 157(1-3), 11–14 (2009).
[Crossref]

Balasubramanian, G.

J. P. Boudou, P. A. Curmi, F. Jelezko, J. Wrachtrup, P. Aubert, M. Sennour, G. Balasubramanian, R. Reuter, A. Thorel, and E. Gaffet, “High yield fabrication of fluorescent nanodiamonds,” Nanotechnology 20(23), 235602 (2009).
[Crossref]

Bao, X.

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L. Basso, F. Gorrini, N. Bazzanella, M. Cazzanelli, C. Dorigoni, A. Bifone, and A. Miotello, “The modeling and synthesis of nanodiamonds by laser ablation of graphite and diamond-like carbon in liquid-confined ambient,” Appl. Phys. A: Mater. Sci. Process. 124(1), 72 (2018).
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H.-B. Jiang, Y.-L. Zhang, Y. Liu, X.-Y. Fu, Y.-F. Li, Y.-Q. Liu, C.-H. Li, and H.-B. Sun, “Bioinspired few-layer graphene prepared by chemical vapor deposition on femtosecond laser-structured Cu foil,” Laser Photonics Rev. 10(3), 441–450 (2016).
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L. Jiang, A. D. Wang, B. Li, T. H. Cui, and Y. F. Lu, “Electrons dynamics control by shaping femtosecond laser pulses in micro/nanofabrication: modeling, method, measurement and application,” Light: Sci. Appl. 7(2), 17134 (2018).
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D. Amans, A. C. Chenus, G. Ledoux, C. Dujardin, C. Reynaud, O. Sublemontier, K. Masenelli-Varlot, and O. Guillois, “Nanodiamond synthesis by pulsed laser ablation in liquids,” Diamond Relat. Mater. 18(2-3), 177–180 (2009).
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C. Doñate-Buendía, M. Fernández-Alonso, J. Lancis, and G. Mínguez-Vega, “Overcoming the barrier of nanoparticle production by femtosecond laser ablation in liquids using simultaneous spatial and temporal focusing,” Photonics Res. 7(11), 1249 (2019).
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M. I. Setyawati, V. N. Mochalin, and D. T. Leong, “Tuning Endothelial Permeability with Functionalized Nanodiamonds,” ACS Nano 10(1), 1170–1181 (2016).
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V. N. Mochalin, O. Shenderova, D. Ho, and Y. Gogotsi, “The properties and applications of nanodiamonds,” Nat. Nanotechnol. 7(1), 11–23 (2012).
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S. Han, S. G. Prussin, J. W. Ager, L. S. Pan, D. R. Kania, S. M. Lane, and R. S. Wagner, “Radiation-Damage Study of Polycrystalline Cvd and Natural Type-Iia Diamonds Using Raman and Photoluminescence Spectroscopies,” Nucl. Instrum. Methods Phys. Res., Sect. B 80-81(1), 1446–1450 (1993).
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X. B. Cheng, M. Q. Zhao, C. Chen, A. Pentecost, K. Maleski, T. Mathis, X. Q. Zhang, Q. Zhang, J. Jiang, and Y. Gogotsi, “Nanodiamonds suppress the growth of lithium dendrites,” Nat. Commun. 8(1), 336 (2017).
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Figures (4)

Fig. 1.
Fig. 1. a) The synthetic scheme of NDs by fs-PLAL and process of surface passivation treatment. b) TEM image of NDs. c) HRTEM image of NDs. d) Size distribution of NDs. e) NDs colloid solution after surface passivation under natural light (left) and the emission photo irradiated by 343 nm laser (right).
Fig. 2.
Fig. 2. a) Raman spectra of NDs and bulk diamond; b) FTIR spectra of NDs with and without passivation.
Fig. 3.
Fig. 3. a) UV-Vis absorption spectra and b) ablation efficiency and absorption peak position of NDs fabricated by fs-PLAL method under different laser power.
Fig. 4.
Fig. 4. The emission spectra of a) un-passivated and b) passivated NDs excited by 260 nm and 280 nm; The emission spectra of c) un-passivated NDs and d) passivated NDs excited by 320 nm ∼ 420 nm.

Equations (1)

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λ g = 1240 × E g 1