Abstract

Benefiting from high-performance of photoelectric, hybrid organic-inorganic perovskite shows great development potential. We introduce a composite nanostructure of monolayer well-organized mesoporous silica, with a wrapped silver nanowire as a core. A gain material, methyl ammonium lead bromide (MAPbBr3) was embedded in mesoporous silica (mSiO2). Using 400-nm and 800-nm femtosecond lasers for pumping, which were corresponding to one-photon and two-photon regimes, the laser sign peaks appeared at 549 nm and 546 nm. The amplified spontaneous emissions (ASE) were observed, as well, giant enhancements of ASE can be obtained due to the localized field of surface plasmon resonance caused by silver-core. Compared with composites without silver nanowire cores to enhance the field distribution, the thresholds are significantly down to ∼62% and 32% of original values under 400-nm and 800-nm femtosecond lasers pump, respectively.

© 2020 Optical Society of America under the terms of the OSA Open Access Publishing Agreement

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    [Crossref]
  28. M. Olejnik, B. Krajnik, D. Kowalska, M. Twardowska, N. Czechowski, E. Hofmann, and S. Mackowski, “Imaging of fluorescence enhancement in photosynthetic complexes coupled to silver nanowires,” Appl. Phys. Lett. 102(8), 083703 (2013).
    [Crossref]
  29. B. Wild, L. Cao, Y. Sun, B. P. Khanal, E. R. Zubarev, S. K. Gray, N. F. Scherer, and M. Pelton, “Propagation Lengths and Group Velocities of Plasmons in Chemically Synthesized Gold and Silver Nanowires,” ACS Nano 6(1), 472–482 (2012).
    [Crossref]
  30. B. Wang, L. Ma, C. Sun, Z. Cheng, W. Gui, and C. Cheng, “Solid-state optoelectronic device based on TiO2/SnSe2 core-shell nanocable structure,” Opt. Mater. Express 7(10), 3691–3696 (2017).
    [Crossref]
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    [Crossref]
  32. W. Park, D. Lu, and S. Ahn, “C,” Chem. Soc. Rev. 44(10), 2940–2962 (2015).
    [Crossref]
  33. J. Yang, F. Zhang, Y. Chen, S. Qian, P. Hu, W. Li, Y. H. Deng, Y. Fang, L. Han, M. Luqman, and D. Y. Zhao, “Core-shell Ag@SiO2@mSiO2 mesoporous nanocarriers for metal-enhanced fluorescence,” Chem. Commun. 47(42), 11618 (2011).
    [Crossref]
  34. T. H. Elmer and M. E. Nordberg, “Solubility of Silica in Nitric Acid Solutions,” J. Am. Ceram. Soc. 41(12), 517–520 (1958).
    [Crossref]
  35. C. Özmetin, M. Çopur, A. Yartasi, and M. M. Kocakerim, “Kinetic Investigation of Reaction Between Metallic Silver and Nitric Acid Solutions,” Chem. Eng. Technol. 23(8), 707–711 (2000).
    [Crossref]
  36. K. Xu, J.-X. Wang, X.-L. Kang, and J.-F. Chen, “Fabrication of antibacterial monodispersed Ag–SiO2 core–shell nanoparticles with high concentration,” Mater. Lett. 63(1), 31–33 (2009).
    [Crossref]
  37. L. M. Liz-Marzán, M. Giersig, and P. Mulvaney, “Synthesis of Nanosized Gold−Silica Core−Shell Particles,” Langmuir 12(18), 4329–4335 (1996).
    [Crossref]
  38. Y. Jiang, X. Wang, and A. Pan, “Properties of Excitons and Photogenerated Charge Carriers in Metal Halide Perovskites,” Adv. Mater. 31(47), 1806671 (2019).
    [Crossref]
  39. F. Chen, C. Xu, Q. Xu, Y. Zhu, R. Wang, J. Zhao, X. Wang, M. Chen, and F. Qin, “Detachable surface plasmon substrate to enhance CH3NH3PbBr3 lasing,” Opt. Commun. 452(1), 400–404 (2019).
    [Crossref]
  40. X. Wu, Y. Li, W. Li, L. Wu, B. Fu, W. Wang, G. Liu, D. Zhang, J. Zhao, and P. Chen, “Enhancing Optically Pumped Organic-Inorganic Hybrid Perovskite Amplified Spontaneous Emission via Compound Surface Plasmon Resonance,” Crystals 8(3), 124 (2018).
    [Crossref]
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    [Crossref]

2019 (8)

S. A. Kulkarni, S. G. Mhaisalkar, N. Mathews, and P. P. Boix, “Perovskite Nanoparticles: Synthesis, Properties, and Novel Applications in Photovoltaics and LEDs,” Small Methods 3(1), 1800231 (2019).
[Crossref]

M. Han, J. Sun, M. Peng, N. Han, Z. Chen, D. Liu, Y. Guo, S. Zhao, C. Shan, T. Xu, X. Hao, W. Hu, and Z. Yang, “Controllable Growth of Lead-Free All-Inorganic Perovskite Nanowires Array with Fast and Stable Near-Infrared Photodetection,” J. Phys. Chem. C 123(28), 17566–17573 (2019).
[Crossref]

W. Ruan, Z. Zhang, Y. Hu, F. Bai, T. Qiu, and S. Zhang, “Self-passivated perovskite solar cells with wider bandgap perovskites as electron blocking layer,” Appl. Surf. Sci. 465(28), 420–426 (2019).
[Crossref]

D. Gets, D. Saranin, A. Ishteev, R. Haroldson, E. Danilovskiy, S. Makarov, and A. Zakhidov, “Light-Emitting Perovskite Solar Cell with Segregation Enhanced Self Doping,” Appl. Surf. Sci. 476(15), 486–492 (2019).
[Crossref]

C. Li, Z. Liu, Q. Shang, and Q. Zhang, “Surface-Plasmon-Assisted Metal Halide Perovskite Small Lasers,” Adv. Opt. Mater. 7(17), 1900279 (2019).
[Crossref]

J. Yang, Z. Liu, Z. Hu, F. Zeng, Z. Zhang, Y. Yao, Z. Yao, X. Tang, J. Du, Z. Zang, M. Pi, L. Liu, and Y. Leng, “Enhanced Single-Mode Lasers of All-Inorganic Perovskite Nanocube by Localized Surface Plasmonic Effect from Au Nanoparticles,” J. Lumin. 208, 402–407 (2019).
[Crossref]

Y. Jiang, X. Wang, and A. Pan, “Properties of Excitons and Photogenerated Charge Carriers in Metal Halide Perovskites,” Adv. Mater. 31(47), 1806671 (2019).
[Crossref]

F. Chen, C. Xu, Q. Xu, Y. Zhu, R. Wang, J. Zhao, X. Wang, M. Chen, and F. Qin, “Detachable surface plasmon substrate to enhance CH3NH3PbBr3 lasing,” Opt. Commun. 452(1), 400–404 (2019).
[Crossref]

2018 (8)

X. Wu, Y. Li, W. Li, L. Wu, B. Fu, W. Wang, G. Liu, D. Zhang, J. Zhao, and P. Chen, “Enhancing Optically Pumped Organic-Inorganic Hybrid Perovskite Amplified Spontaneous Emission via Compound Surface Plasmon Resonance,” Crystals 8(3), 124 (2018).
[Crossref]

Z. Liu, J. Yang, J. Du, Z. Hu, T. Shi, Z. Zhang, Y. Liu, X. Tang, Y. Leng, and R. Li, “Robust subwavelength single-mode perovskite nanocuboid laser,” ACS Nano 12(6), 5923–5931 (2018).
[Crossref]

Q. Shang, S. Zhang, Z. Liu, J. Chen, P. Yang, C. Li, W. Li, Y. Zhang, Q. Xiong, X. Liu, and Q. Zhang, “Surface Plasmon Enhanced Strong Exciton–Photon Coupling in Hybrid Inorganic–Organic Perovskite Nanowires,” Nano Lett. 18(6), 3335–3343 (2018).
[Crossref]

Y. Meng, X. Wu, Z. Xiong, C. Lin, Z. Xiong, E. Blount, and P. Chen, “Electrode quenching control for highly efficient CsPbBr3 perovskite light-emitting diodes via surface plasmon resonance and enhanced hole injection by Au nanoparticles,” Nanotechnology 29(17), 175203 (2018).
[Crossref]

X. Wu, Y. Li, W. Li, L. Wu, B. Fu, W. Wang, G. Liu, D. Zhang, J. Zhao, and P. Chen, “Enhancing Optically Pumped Organic-Inorganic Hybrid Perovskite Amplified Spontaneous Emission via Compound Surface Plasmon Resonance,” Crystals 8(3), 124 (2018).
[Crossref]

H. Hu, F. Meier, D. Zhao, Y. Abe, Y. Gao, B. Chen, E. Salim, E. M. Chia, X. Qiao, C. Deibel, and Y. M. Lam, “Efficient Room-Temperature Phosphorescence from Organic-Inorganic Hybrid Perovskites by Molecular Engineering,” Adv. Mater. 30(36), 1707621 (2018).
[Crossref]

G. Jia, Z.-J. Shi, Y.-D. Xia, Q. Wei, Y.-H. Chen, G.-C. Xing, and W. Huang, “Super air stable quasi-2D organic-inorganic hybrid perovskites for visible light-emitting diodes,” Opt. Express 26(2), A66 (2018).
[Crossref]

H. Tsai, W. Nie, J.-C. Blancon, C. C. Stoumpos, C. M. M. Soe, J. Yoo, J. Crochet, S. Tretiak, J. Even, A. Sadhanala, G. Azzellino, R. Brenes, P. M. Ajayan, V. Bulović, S. D. Stranks, R. H. Friend, M. G. Kanatzidis, and A. D. Mohite, “Stable Light-Emitting Diodes Using Phase-Pure Ruddlesden-Popper Layered Perovskites,” Adv. Mater. 30(6), 1704217 (2018).
[Crossref]

2017 (4)

J.-W. Xiao, L. Liu, D. Zhang, N. De Marco, J.-W. Lee, O. Lin, Q. Chen, and Y. Yang, “The Emergence of the Mixed Perovskites and Their Applications as Solar Cells,” Adv. Energy Mater. 7(20), 1700491 (2017).
[Crossref]

S. Ye, M. Yu, W. Yan, J. Song, and J. Qu, “Enhanced photoluminescence of CsPbBr3@Ag hybrid perovskite quantum dots,” J. Mater. Chem. C 5(32), 8187–8193 (2017).
[Crossref]

L. Xu, Y. Qiang, K. Xiao, Y. Zhang, J. Xie, C. Cui, P. Lin, P. Wang, X. Yu, F. Wu, and D. Yang, “Surface plasmon enhanced luminescence from organic-inorganic hybrid perovskites,” Appl. Phys. Lett. 110(23), 233113 (2017).
[Crossref]

B. Wang, L. Ma, C. Sun, Z. Cheng, W. Gui, and C. Cheng, “Solid-state optoelectronic device based on TiO2/SnSe2 core-shell nanocable structure,” Opt. Mater. Express 7(10), 3691–3696 (2017).
[Crossref]

2016 (5)

S. Liu, L. Wang, W.-C. Lin, S. Sucharitakul, C. Burda, and X. P. A. Gao, “Imaging the Long Transport Lengths of Photo-generated Carriers in Oriented Perovskite Films,” Nano Lett. 16(12), 7925–7929 (2016).
[Crossref]

E. J. Juarez-Perez, Z. Hawash, S. R. Raga, L. K. Ono, and Y. Qi, “Thermal degradation of CH3NH3PbI3 perovskite into NH3 and CH3I gases observed by coupled thermogravimetry–mass spectrometry analysis,” Energy Environ. Sci. 9(11), 3406–3410 (2016).
[Crossref]

N. H. Tiep, Z. Ku, and H. J. Fan, “Recent Advances in Improving the Stability of Perovskite Solar Cells,” Adv. Energy Mater. 6(3), 1501420 (2016).
[Crossref]

V. Malgras, S. Tominaka, J. W. Ryan, J. Henzie, T. Takei, K. Ohara, and Y. Yamauchi, “Observation of Quantum Confinement in Monodisperse Methylammonium Lead Halide Perovskite Nanocrystals Embedded in Mesoporous Silica,” J. Am. Chem. Soc. 138(42), 13874–13881 (2016).
[Crossref]

T. S. Kao, K.-B. Hong, Y.-H. Chou, J.-F. Huang, F.-C. Chen, and T.-C. Lu, “Localized surface plasmon for enhanced lasing performance in solution-processed perovskites,” Opt. Express 24(18), 20696 (2016).
[Crossref]

2015 (6)

H. Huang, A. S. Susha, S. V. Kershaw, T. F. Hung, and A. L. Rogach, “Control of Emission Color of High Quantum Yield MAPbBr3 Perovskite Quantum Dots by Precipitation Temperature,” Adv. Sci. 2(9), 1500194 (2015).
[Crossref]

T. C. Sum, S. Chen, G. Xing, X. Liu, and B. Wu, “Energetics and dynamics in organic–inorganic halide perovskite photovoltaics and light emitters,” Nanotechnology 26(34), 342001 (2015).
[Crossref]

S. D. Stranks and H. J. Snaith, “Metal-halide perovskites for photovoltaic and light-emitting devices,” Nat. Nanotechnol. 10(5), 391–402 (2015).
[Crossref]

Q. Liao, K. Hu, H. Zhang, X. Wang, J. Yao, and H. Fu, “Perovskite Microdisk Microlasers Self-Assembled from Solution,” Adv. Mater. 27(22), 3405–3410 (2015).
[Crossref]

Q. Dong, Y. Fang, Y. Shao, P. Mulligan, J. Qiu, L. Cao, and J. Huang, “Electron-hole diffusion lengths > 175 μm in solution-grown CH3NH3PbI3 single crystals,” Science 347(6225), 967–970 (2015).
[Crossref]

W. Park, D. Lu, and S. Ahn, “C,” Chem. Soc. Rev. 44(10), 2940–2962 (2015).
[Crossref]

2014 (1)

G. Xing, N. Mathews, S. S. Lim, N. Yantara, X. Liu, D. Sabba, M. Grätzel, S. Mhaisalkar, and T. C. Sum, “Low-temperature solution-processed wavelength-tunable perovskites for lasing,” Nat. Mater. 13(5), 476–480 (2014).
[Crossref]

2013 (1)

M. Olejnik, B. Krajnik, D. Kowalska, M. Twardowska, N. Czechowski, E. Hofmann, and S. Mackowski, “Imaging of fluorescence enhancement in photosynthetic complexes coupled to silver nanowires,” Appl. Phys. Lett. 102(8), 083703 (2013).
[Crossref]

2012 (2)

B. Wild, L. Cao, Y. Sun, B. P. Khanal, E. R. Zubarev, S. K. Gray, N. F. Scherer, and M. Pelton, “Propagation Lengths and Group Velocities of Plasmons in Chemically Synthesized Gold and Silver Nanowires,” ACS Nano 6(1), 472–482 (2012).
[Crossref]

M. M. Lee, J. Teuscher, T. Miyasaka, T. N. Murakami, and H. J. Snaith, “Efficient Hybrid Solar Cells Based on Meso-Superstructured Organometal Halide Perovskites,” Science 338(6107), 643–647 (2012).
[Crossref]

2011 (1)

J. Yang, F. Zhang, Y. Chen, S. Qian, P. Hu, W. Li, Y. H. Deng, Y. Fang, L. Han, M. Luqman, and D. Y. Zhao, “Core-shell Ag@SiO2@mSiO2 mesoporous nanocarriers for metal-enhanced fluorescence,” Chem. Commun. 47(42), 11618 (2011).
[Crossref]

2009 (1)

K. Xu, J.-X. Wang, X.-L. Kang, and J.-F. Chen, “Fabrication of antibacterial monodispersed Ag–SiO2 core–shell nanoparticles with high concentration,” Mater. Lett. 63(1), 31–33 (2009).
[Crossref]

2000 (1)

C. Özmetin, M. Çopur, A. Yartasi, and M. M. Kocakerim, “Kinetic Investigation of Reaction Between Metallic Silver and Nitric Acid Solutions,” Chem. Eng. Technol. 23(8), 707–711 (2000).
[Crossref]

1996 (2)

L. M. Liz-Marzán, M. Giersig, and P. Mulvaney, “Synthesis of Nanosized Gold−Silica Core−Shell Particles,” Langmuir 12(18), 4329–4335 (1996).
[Crossref]

A. P. Alivisatos, “Semiconductor Clusters, Nanocrystals, and Quantum Dots,” Science 271(5251), 933–937 (1996).
[Crossref]

1958 (1)

T. H. Elmer and M. E. Nordberg, “Solubility of Silica in Nitric Acid Solutions,” J. Am. Ceram. Soc. 41(12), 517–520 (1958).
[Crossref]

Abe, Y.

H. Hu, F. Meier, D. Zhao, Y. Abe, Y. Gao, B. Chen, E. Salim, E. M. Chia, X. Qiao, C. Deibel, and Y. M. Lam, “Efficient Room-Temperature Phosphorescence from Organic-Inorganic Hybrid Perovskites by Molecular Engineering,” Adv. Mater. 30(36), 1707621 (2018).
[Crossref]

Ahn, S.

W. Park, D. Lu, and S. Ahn, “C,” Chem. Soc. Rev. 44(10), 2940–2962 (2015).
[Crossref]

Ajayan, P. M.

H. Tsai, W. Nie, J.-C. Blancon, C. C. Stoumpos, C. M. M. Soe, J. Yoo, J. Crochet, S. Tretiak, J. Even, A. Sadhanala, G. Azzellino, R. Brenes, P. M. Ajayan, V. Bulović, S. D. Stranks, R. H. Friend, M. G. Kanatzidis, and A. D. Mohite, “Stable Light-Emitting Diodes Using Phase-Pure Ruddlesden-Popper Layered Perovskites,” Adv. Mater. 30(6), 1704217 (2018).
[Crossref]

Alivisatos, A. P.

A. P. Alivisatos, “Semiconductor Clusters, Nanocrystals, and Quantum Dots,” Science 271(5251), 933–937 (1996).
[Crossref]

Azzellino, G.

H. Tsai, W. Nie, J.-C. Blancon, C. C. Stoumpos, C. M. M. Soe, J. Yoo, J. Crochet, S. Tretiak, J. Even, A. Sadhanala, G. Azzellino, R. Brenes, P. M. Ajayan, V. Bulović, S. D. Stranks, R. H. Friend, M. G. Kanatzidis, and A. D. Mohite, “Stable Light-Emitting Diodes Using Phase-Pure Ruddlesden-Popper Layered Perovskites,” Adv. Mater. 30(6), 1704217 (2018).
[Crossref]

Bai, F.

W. Ruan, Z. Zhang, Y. Hu, F. Bai, T. Qiu, and S. Zhang, “Self-passivated perovskite solar cells with wider bandgap perovskites as electron blocking layer,” Appl. Surf. Sci. 465(28), 420–426 (2019).
[Crossref]

Blancon, J.-C.

H. Tsai, W. Nie, J.-C. Blancon, C. C. Stoumpos, C. M. M. Soe, J. Yoo, J. Crochet, S. Tretiak, J. Even, A. Sadhanala, G. Azzellino, R. Brenes, P. M. Ajayan, V. Bulović, S. D. Stranks, R. H. Friend, M. G. Kanatzidis, and A. D. Mohite, “Stable Light-Emitting Diodes Using Phase-Pure Ruddlesden-Popper Layered Perovskites,” Adv. Mater. 30(6), 1704217 (2018).
[Crossref]

Blount, E.

Y. Meng, X. Wu, Z. Xiong, C. Lin, Z. Xiong, E. Blount, and P. Chen, “Electrode quenching control for highly efficient CsPbBr3 perovskite light-emitting diodes via surface plasmon resonance and enhanced hole injection by Au nanoparticles,” Nanotechnology 29(17), 175203 (2018).
[Crossref]

Boix, P. P.

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G. Xing, N. Mathews, S. S. Lim, N. Yantara, X. Liu, D. Sabba, M. Grätzel, S. Mhaisalkar, and T. C. Sum, “Low-temperature solution-processed wavelength-tunable perovskites for lasing,” Nat. Mater. 13(5), 476–480 (2014).
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H. Hu, F. Meier, D. Zhao, Y. Abe, Y. Gao, B. Chen, E. Salim, E. M. Chia, X. Qiao, C. Deibel, and Y. M. Lam, “Efficient Room-Temperature Phosphorescence from Organic-Inorganic Hybrid Perovskites by Molecular Engineering,” Adv. Mater. 30(36), 1707621 (2018).
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C. Li, Z. Liu, Q. Shang, and Q. Zhang, “Surface-Plasmon-Assisted Metal Halide Perovskite Small Lasers,” Adv. Opt. Mater. 7(17), 1900279 (2019).
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Q. Shang, S. Zhang, Z. Liu, J. Chen, P. Yang, C. Li, W. Li, Y. Zhang, Q. Xiong, X. Liu, and Q. Zhang, “Surface Plasmon Enhanced Strong Exciton–Photon Coupling in Hybrid Inorganic–Organic Perovskite Nanowires,” Nano Lett. 18(6), 3335–3343 (2018).
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Z. Liu, J. Yang, J. Du, Z. Hu, T. Shi, Z. Zhang, Y. Liu, X. Tang, Y. Leng, and R. Li, “Robust subwavelength single-mode perovskite nanocuboid laser,” ACS Nano 12(6), 5923–5931 (2018).
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Figures (10)

Fig. 1.
Fig. 1. SEM images of the (a) Ag@mSiO2 and (inset) Ag nanowires. TEM (b) images of the magnified interface of Ag and mSiO2, inset is the magnified Ag@mSiO2 nanowire viewed in hundred-nanometer-scale.
Fig. 2.
Fig. 2. (a) Normalized optical density spectrum of different composite materials. (b) PL spectrum of different composite materials under 400 nm pumped emission.
Fig. 3.
Fig. 3. The measured spectroscopy of (a) Ag@mSiO2/MAPbBr3 NWs and (c) mSiO2/MAPbBr3 NWs films; The ASE threshold and FWHM behaviors of (b) Ag@mSiO2/MAPbBr3 NWs and (d) mSiO2/MAPbBr3 NWs films.
Fig. 4.
Fig. 4. Emission spectra of samples with/without Ag nanowire cores under (a) 400 nm and (b) 800 nm femtosecond laser (2.2 μJ/pulse and 3.4 μJ/pulse pumped emission respectively).
Fig. 5.
Fig. 5. The field intensity distributions of cross-section of the two structures at 400 nm (a) with and (b) without silver cores, respectively.
Fig. 6.
Fig. 6. Photostability of PL intensity of the Ag@mSiO2/MAPbBr3 nanowires under 400 nm pumped emission (2.8 μJ/pulse).
Fig. 7.
Fig. 7. A schematic representation of preparation process of the Ag@mSiO2/MAPbBr3 composite structure.
Fig. 8.
Fig. 8. EDS spectrum and EDS element mapping images (inset) of Ag@mSiO2 nanowires.
Fig. 9.
Fig. 9. (a) Dark field images of the Ag@mSiO2 nanowires and (inset) the Ag nanowires. (b) Pore size distribution and N2.
Fig. 10.
Fig. 10. The measured spectra of nano composites (a) with and (b) without silver cores under 800 nm pumped emission, respectively.