Abstract

Plasmonic resonances in metallic nanostructures are promising for the structure-dependent color-rendering effect. In this study, bismuth is selected as an alternative plasmonic material due to its large tunable range from near-ultraviolet to near-infrared. Various sizes of core-shell bismuth nanoparticles are fabricated on a large-area silicon substrate using a one-step thermal evaporation deposition process. Particle diameters, cross-sections, and arrangement are characterized at 12 featured sections, which reveal spectral shifts and full visible colors in a hue order with a color gamut that is close to sRGB. Color palettes on the chromaticity coordinates rendered from both measured and simulation reflection spectra are in very good accordance with the microscopic image colors of all sections.

© 2020 Optical Society of America under the terms of the OSA Open Access Publishing Agreement

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2020 (1)

2019 (3)

A. Ghobadi, H. Hajian, M. Gokbayrak, B. Butun, and E. Ozbay, “Bismuth-based metamaterials: from narrowband reflective color filter to extremely broadband near perfect absorber,” Nanophotonics 8(5), 823–832 (2019).
[Crossref]

H. Nishi and T. Tatsuma, “Full-color scattering based on plasmon and Mie resonances of gold nanoparticles modulated by Fabry–Pérot interference for coloring and image projection,” ACS Appl. Nano Mater. 2(8), 5071–5078 (2019).
[Crossref]

S. D. Rezaei, R. J. Hong Ng, Z. Dong, J. Ho, E. H. H. Koay, S. Ramakrishna, and J. K. W. Yang, “Wide-gamut plasmonic color palettes with constant subwavelength resolution,” ACS Nano 13(3), 3580–3588 (2019).
[Crossref]

2018 (1)

2017 (4)

J. Toudert and R. Serna, “Interband transitions in semi-metals, semiconductors, and topological insulators: a new driving force for plasmonics and nanophotonics [Invited],” Opt. Mater. Express 7(7), 2299–2325 (2017).
[Crossref]

J. Toudert, R. Serna, I. Camps, J. Wojcik, P. Mascher, E. Rebollar, and T. A. Ezquerra, “Unveiling the far infrared-to-ultraviolet optical properties of bismuth for applications in plasmonics and nanophotonics,” J. Phys. Chem. C 121(6), 3511–3521 (2017).
[Crossref]

A. Kristensen, J. K. W. Yang, S. I. Bozhevolnyi, S. Link, P. Nordlander, N. J. Halas, and N. A. Mortensen, “Plasmonic colour generation,” Nat. Rev. Mater. 2(1), 16088 (2017).
[Crossref]

A. Reyes-Contreras, M. Camacho-López, S. Camacho-López, O. Olea-Mejía, A. Esparza-García, J. G. Bañuelos-Muñetón, and M. A. Camacho-López, “Laser-induced periodic surface structures on bismuth thin films with ns laser pulses below ablation threshold,” Opt. Mater. Express 7(6), 1777–1786 (2017).
[Crossref]

2016 (9)

J. Olson, A. Manjavacas, T. Basu, D. Huang, A. E. Schlather, B. Zheng, N. J. Halas, P. Nordlander, and S. Link, “High chromaticity aluminum plasmonic pixels for active liquid crystal displays,” ACS Nano 10(1), 1108–1117 (2016).
[Crossref]

M. Tanzid, A. Sobhani, C. J. DeSantis, Y. Cui, N. J. Hogan, A. Samaniego, A. Veeraraghavan, and N. J. Halas, “Imaging through plasmonic nanoparticles,” Proc. Natl. Acad. Sci. U. S. A. 113(20), 5558–5563 (2016).
[Crossref]

R. Yu, P. Mazumder, N. F. Borrelli, A. Carrilero, D. S. Ghosh, R. A. Maniyara, D. Baker, F. J. García de Abajo, and V. Pruneri, “Structural coloring of glass using dewetted nanoparticles and ultrathin films of metals,” ACS Photonics 3(7), 1194–1201 (2016).
[Crossref]

L. Sun, X. Hu, Q. Wu, L. Wang, J. Zhao, S. Yang, R. Tai, H. J. Fecht, D. X. Zhang, L. Q. Wang, and J. Z. Jiang, “High throughput fabrication of large-area plasmonic color filters by soft-X-ray interference lithography,” Opt. Express 24(17), 19112–19121 (2016).
[Crossref]

X. Zhu, C. Vannahme, E. Hojlund-Nielsen, N. A. Mortensen, and A. Kristensen, “Plasmonic colour laser printing,” Nat. Nanotechnol. 11(4), 325–329 (2016).
[Crossref]

Y. Gutierrez, D. Ortiz, J. M. Sanz, J. M. Saiz, F. Gonzalez, H. O. Everitt, and F. Moreno, “How an oxide shell affects the ultraviolet plasmonic behavior of Ga, Mg, and Al nanostructures,” Opt. Express 24(18), 20621–20631 (2016).
[Crossref]

L. Wang, R. J. H. Ng, S. Safari Dinachali, M. Jalali, Y. Yu, and J. K. W. Yang, “Large area plasmonic color palettes with expanded gamut using colloidal self-assembly,” ACS Photonics 3(4), 627–633 (2016).
[Crossref]

J. Toudert and R. Serna, “Ultraviolet-visible interband plasmonics with p-block elements,” Opt. Mater. Express 6(7), 2434–2447 (2016).
[Crossref]

A. Cuadrado, J. Toudert, and R. Serna, “Polaritonic-to-plasmonic transition in optically resonant bismuth nanospheres for high-contrast switchable ultraviolet meta-filters,” IEEE Photonics J. 8(3), 1–11 (2016).
[Crossref]

2015 (7)

J. D. Yao, J. M. Shao, and G. W. Yang, “Ultra-broadband and high-responsive photodetectors based on bismuth film at room temperature,” Sci. Rep. 5(1), 12320 (2015).
[Crossref]

A. Sobhani, A. Manjavacas, Y. Cao, M. J. McClain, F. J. Garcia de Abajo, P. Nordlander, and N. J. Halas, “Pronounced linewidth narrowing of an aluminum nanoparticle plasmon resonance by interaction with an aluminum metallic film,” Nano Lett. 15(10), 6946–6951 (2015).
[Crossref]

J. Olson, S. Dominguez-Medina, A. Hoggard, L. Y. Wang, W. S. Chang, and S. Link, “Optical characterization of single plasmonic nanoparticles,” Chem. Soc. Rev. 44(1), 40–57 (2015).
[Crossref]

M. W. Knight, T. Coenen, Y. Yang, B. J. M. Brenny, M. Losurdo, A. S. Brown, H. O. Everitt, and A. Polman, “Gallium plasmonics: deep subwavelength spectroscopic imaging of single and interacting gallium nanoparticles,” ACS Nano 9(2), 2049–2060 (2015).
[Crossref]

F. Khalilzadeh-Rezaie, C. W. Smith, J. Nath, N. Nader, M. Shahzad, J. W. Cleary, I. Avrutsky, and R. E. Peale, “Infrared surface polaritons on bismuth,” J. Nanophotonics 9(1), 093792 (2015).
[Crossref]

N. S. King, L. Liu, X. Yang, B. Cerjan, H. O. Everitt, P. Nordlander, and N. J. Halas, “Fano resonant aluminum nanoclusters for plasmonic colorimetric sensing,” ACS Nano 9(11), 10628–10636 (2015).
[Crossref]

Y. Shen, V. Rinnerbauer, I. Wang, V. Stelmakh, J. D. Joannopoulos, and M. Soljačić, “Structural colors from Fano resonances,” ACS Photonics 2(1), 27–32 (2015).
[Crossref]

2014 (8)

J. Olson, A. Manjavacas, L. Liu, W. S. Chang, B. Foerster, N. S. King, M. W. Knight, P. Nordlander, N. J. Halas, and S. Link, “Vivid, full-color aluminum plasmonic pixels,” Proc. Natl. Acad. Sci. U. S. A. 111(40), 14348–14353 (2014).
[Crossref]

J. A. Steele and R. A. Lewis, “In situ micro-Raman studies of laser-induced bismuth oxidation reveals metastability of β-Bi2O3 microislands,” Opt. Mater. Express 4(10), 2133–2142 (2014).
[Crossref]

S. J. Tan, L. Zhang, D. Zhu, X. M. Goh, Y. M. Wang, K. Kumar, C. W. Qiu, and J. K. Yang, “Plasmonic color palettes for photorealistic printing with aluminum nanostructures,” Nano Lett. 14(7), 4023–4029 (2014).
[Crossref]

V. R. Shrestha, S. S. Lee, E. S. Kim, and D. Y. Choi, “Aluminum plasmonics based highly transmissive polarization-independent subtractive color filters exploiting a nanopatch array,” Nano Lett. 14(11), 6672–6678 (2014).
[Crossref]

Y. Kumamoto, A. Taguchi, M. Honda, K. Watanabe, Y. Saito, and S. Kawata, “Indium for deep-ultraviolet surface-enhanced resonance Raman scattering,” ACS Photonics 1(7), 598–603 (2014).
[Crossref]

U. Zywietz, A. B. Evlyukhin, C. Reinhardt, and B. N. Chichkov, “Laser printing of silicon nanoparticles with resonant optical electric and magnetic responses,” Nat. Commun. 5(1), 3402 (2014).
[Crossref]

F. Dong, T. Xiong, Y. Sun, Z. Zhao, Y. Zhou, X. Feng, and Z. Wu, “A semimetal bismuth element as a direct plasmonic photocatalyst,” Chem. Commun. 50(72), 10386–10389 (2014).
[Crossref]

M. Jiménez de Castro, F. Cabello, J. Toudert, R. Serna, and E. Haro-Poniatowski, “Potential of bismuth nanoparticles embedded in a glass matrix for spectral-selective thermo-optical devices,” Appl. Phys. Lett. 105(11), 113102 (2014).
[Crossref]

2013 (3)

J. M. McMahon, G. C. Schatz, and S. K. Gray, “Plasmonics in the ultraviolet with the poor metals Al, Ga, In, Sn, Tl, Pb, and Bi,” Phys. Chem. Chem. Phys. 15(15), 5415–5423 (2013).
[Crossref]

Y. H. Fu, A. I. Kuznetsov, A. E. Miroshnichenko, Y. F. Yu, and B. Luk’yanchuk, “Directional visible light scattering by silicon nanoparticles,” Nat. Commun. 4(1), 1527 (2013).
[Crossref]

Y. Yang, J. M. Callahan, T. H. Kim, A. S. Brown, and H. O. Everitt, “Ultraviolet nanoplasmonics: a demonstration of surface-enhanced Raman spectroscopy, fluorescence, and photodegradation using gallium nanoparticles,” Nano Lett. 13(6), 2837–2841 (2013).
[Crossref]

2012 (4)

I. Ament, J. Prasad, A. Henkel, S. Schmachtel, and C. Sonnichsen, “Single unlabeled protein detection on individual plasmonic nanoparticles,” Nano Lett. 12(2), 1092–1095 (2012).
[Crossref]

J. Toudert, R. Serna, and M. Jiménez de Castro, “Exploring the optical potential of nano-bismuth: tunable surface plasmon resonances in the near ultraviolet-to-near infrared range,” J. Phys. Chem. C 116(38), 20530–20539 (2012).
[Crossref]

A. G. Brolo, “Plasmonics for future biosensors,” Nat. Photonics 6(11), 709–713 (2012).
[Crossref]

K. Kumar, H. Duan, R. S. Hegde, S. C. Koh, J. N. Wei, and J. K. Yang, “Printing colour at the optical diffraction limit,” Nat. Nanotechnol. 7(9), 557–561 (2012).
[Crossref]

2010 (1)

J. A. Fan, C. Wu, K. Bao, J. Bao, R. Bardhan, N. J. Halas, V. N. Manoharan, P. Nordlander, G. Shvets, and F. Capasso, “Self-assembled plasmonic nanoparticle clusters,” Science 328(5982), 1135–1138 (2010).
[Crossref]

2008 (4)

J. N. Anker, W. P. Hall, O. Lyandres, N. C. Shah, J. Zhao, and R. P. V. Duyne, “Biosensing with plasmonic nanosensors,” Nat. Mater. 7(6), 442–453 (2008).
[Crossref]

K. Tanabe, “Field enhancement around metal nanoparticles and nanoshells: a systematic investigation,” J. Phys. Chem. C 112(40), 15721–15728 (2008).
[Crossref]

C. Langhammer, M. Schwind, B. Kasemo, and I. Zorić, “Localized surface plasmon resonance in aluminium nanodisks,” Nano Lett. 8(5), 1461–1471 (2008).
[Crossref]

V. Myroshnychenko, J. Rodriguez-Fernandez, I. Pastoriza-Santos, A. M. Funston, C. Novo, P. Mulvaney, L. M. Liz-Marzan, and F. J. Garcia de Abajo, “Modelling the optical response of gold nanoparticles,” Chem. Soc. Rev. 37(9), 1792–1805 (2008).
[Crossref]

2007 (2)

K. A. Willets and R. P. Van Duyne, “Localized surface plasmon resonance spectroscopy and sensing,” Annu. Rev. Phys. Chem. 58(1), 267–297 (2007).
[Crossref]

J. Henzie, M. H. Lee, and T. W. Odom, “Multiscale patterning of plasmonic metamaterials,” Nat. Nanotechnol. 2(9), 549–554 (2007).
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2005 (1)

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ACS Photonics (4)

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Nanophotonics (1)

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Figures (11)

Fig. 1.
Fig. 1. (a) The chamber setup. (b) Fabrication of the Bi NPs on a Si substrate.
Fig. 2.
Fig. 2. Simulation layout of the Bi NPs.
Fig. 3.
Fig. 3. Measurement setup for OM color image and reflection spectrum detection.
Fig. 4.
Fig. 4. SEM pictures of the fabricated Bi NPs under different operation temperature and duration time of thermal evaporation deposition overlaid with diameter statistics. (a) 880 °C, 10 min, (b) 880 °C, 20 min, (c) 880 °C, 30 min, (d) 900 °C, 10 min, (e) 900 °C, 20 min, (f) 900 °C, 30 min, (g) 920 °C, 10 min, (h) 920 °C, 20 min, and (i) 920 °C, 30 min.
Fig. 5.
Fig. 5. (a) Indication of section order on the fabricated sample from center to edge. (b) OM image of the fabricated Bi NPs and the indication of the 12 section indexes. SEM pictures of (c) the 1st (d) the 6th and (e) the 12th featured sections (Scale bar: 400 nm). (f) Particle diameter and gap with the distance from the sample center.
Fig. 6.
Fig. 6. (a) Bi NPs sample cut by FIB and the SEM image of the cross-sectional view at the 1st section (scale bar: 2µm). (b) Particle diameter and film thickness with the distance from the sample center. (Bottom insets: OM image of the sample. Scale bar: 300 µm.) (c) Heights and diameters of a single particle at the 12 sections.
Fig. 7.
Fig. 7. (a) Structural plot of Bi core-shell NPs. (b) Raman scattering spectrum of the fabricated Bi NPs.
Fig. 8.
Fig. 8. (a) Measured reflection spectra and the corresponding OM color images of the fabricated Bi NPs at the featured 12 sections. (b) Measured and (c) simulated reflection spectra at the visible regime (Insets: color palettes from the CIE diagram).
Fig. 9.
Fig. 9. (a) Comparison of CIE color gamut of the fabricated Bi NPs converted from measured reflection spectra with sRGB. (b) The corresponding color palettes on the CIE diagram of the measured spectra (Meas.), measured OM images (OM), and of the simulated spectra (Sim.) of the fabricated Bi NPs at featured 12 sections.
Fig. 10.
Fig. 10. (a) Simulation model of single particle with tuning factors. The simulated reflection spectra of the Bi NP by tuning (b) particle size, (c) oxide shell, (d) film thickness, (e) elliptical aspect ratio, and (f) dewetting film height.
Fig. 11.
Fig. 11. (a) SEM top view (scale bar: 400 nm) and (b) simulation window of the Bi NPs at the 5th section. The corresponding (c) simulated reflection spectrum and the electric fields at resonant wavelengths of (d) 312 nm, (e) 513 nm, and (f) 770 nm.

Tables (2)

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Table 1. Structural parameters of the fabricated Bi NPs

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Table 2. CIE Chromaticity coordinates of the featured 12 sections

Equations (2)

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X = ( S ( λ ) x ¯ ( λ ) ) d λ , Y = ( S ( λ ) y ¯ ( λ ) ) d λ , Z = ( S ( λ ) z ¯ ( λ ) ) d λ
x = X X + Y + Z , y = Y X + Y + Z

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