Abstract

In order to improve the laser-induced damage threshold (LIDT) of the ZrO<sub>2</sub> film, the effect of polyvinyl pyrrolidone (PVP) with different average molecular weight on coatings is studied. The ZrO<sub>2</sub> sol is prepared by the hydrolysis of zirconium n-propoxide with acetylacetone as the chelating agent. The PVP (K16-18) is more suitable to obtain high LIDT coatings than other PVPs. The LIDT of the ZrO<sub>2</sub>-PVP coatings is improved with the increase of the PVP (K16-18) content. When the PVP (K16-18) content is 2.4 wt.-%, the LIDT of the ZrO<sub>2</sub>-PVP coatings is 43.5 J/cm<sup>2</sup> (1064 nm, 12 ns). The ZrO<sub>2</sub> sol and ZrO<sub>2</sub>-PVP (K16-18) sol have the good stability in 3 months. The refractive indices of the ZrO<sub>2</sub>-PVP coatings decrease with the increase of the PVP (K16-18) content.

© 2010 Chinese Optics Letters

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  1. P. M. Pegon, C. V. Germain, Y. R. Rorato, P. F. Belleville, and E. Lavastre, Proc. SPIE 5250, 170 (2004).
  2. D. Grosso and P. A. Sermon, Thin Solid Films 368, 116 (2000).
  3. Y. Guo, X. Zu, X. Jiang, X. Yuan, S. Xu, H. Lv, and B. Wang, Optik 120, 437 (2009).
  4. G. Wang, J. Shen, Z. Xie, G. Wu, and Y. Xiao, Chinese J. Lasers (in Chinese) 33, 380 (2006).
  5. H. Li, Y. Tang, and L. Hu, Acta Opt. Sin. (in Chinese) 29, 558 (2009).
  6. L. Liang, Y. Xu, D. Wu, and Y. Sun, Mater. Chemistry Phys. 114, 252 (2009).
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  10. I. M. Thomas, Proc. SPIE 2288, 50 (1994).
  11. H. Hayashi H. Suzuki, and S. Kaneko, J. Sol-Gel Sci. Technol. 12, 87 (1998).
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  14. I. M. Thomas, Appl. Opt. 31, 6145 (1992).
  15. P. Belleville and P. Pegon, Proc. SPIE 3492, 244 (1999).

2009 (5)

Y. Guo, X. Zu, X. Jiang, X. Yuan, S. Xu, H. Lv, and B. Wang, Optik 120, 437 (2009).

H. Li, Y. Tang, and L. Hu, Acta Opt. Sin. (in Chinese) 29, 558 (2009).

L. Liang, Y. Xu, D. Wu, and Y. Sun, Mater. Chemistry Phys. 114, 252 (2009).

R. Carrion, F. Sittner, C. J. Ochs, S. Flege, and W. Ensinger, Thin Solid Films 517, 1967 (2009).

H. Li, Y. Tang, and L. Hu, Chinese J. Lasers (in Chinese) 36, 472 (2009).

2006 (1)

G. Wang, J. Shen, Z. Xie, G. Wu, and Y. Xiao, Chinese J. Lasers (in Chinese) 33, 380 (2006).

2004 (2)

P. M. Pegon, C. V. Germain, Y. R. Rorato, P. F. Belleville, and E. Lavastre, Proc. SPIE 5250, 170 (2004).

H. Kozuka, S. Takenaka, H. Tokita, and M. Okubayashi, Journal of the European Ceramic Society 24, 1585 (2004).

2000 (1)

D. Grosso and P. A. Sermon, Thin Solid Films 368, 116 (2000).

1999 (1)

P. Belleville and P. Pegon, Proc. SPIE 3492, 244 (1999).

1998 (2)

H. Hayashi H. Suzuki, and S. Kaneko, J. Sol-Gel Sci. Technol. 12, 87 (1998).

N. Bazin, J. E. Andrew, and H. A. Mcinnes, J. Sol-Gel Sci. Technol. 13, 757 (1998).

1994 (2)

H. G. Floch and P. F. Belleville, J. Sol-Gel Sci. Technol. 2, 695 (1994).

I. M. Thomas, Proc. SPIE 2288, 50 (1994).

1992 (1)

Andrew, J. E.

N. Bazin, J. E. Andrew, and H. A. Mcinnes, J. Sol-Gel Sci. Technol. 13, 757 (1998).

Bazin, N.

N. Bazin, J. E. Andrew, and H. A. Mcinnes, J. Sol-Gel Sci. Technol. 13, 757 (1998).

Belleville, P.

P. Belleville and P. Pegon, Proc. SPIE 3492, 244 (1999).

Belleville, P. F.

P. M. Pegon, C. V. Germain, Y. R. Rorato, P. F. Belleville, and E. Lavastre, Proc. SPIE 5250, 170 (2004).

H. G. Floch and P. F. Belleville, J. Sol-Gel Sci. Technol. 2, 695 (1994).

Carrion, R.

R. Carrion, F. Sittner, C. J. Ochs, S. Flege, and W. Ensinger, Thin Solid Films 517, 1967 (2009).

Ensinger, W.

R. Carrion, F. Sittner, C. J. Ochs, S. Flege, and W. Ensinger, Thin Solid Films 517, 1967 (2009).

Flege, S.

R. Carrion, F. Sittner, C. J. Ochs, S. Flege, and W. Ensinger, Thin Solid Films 517, 1967 (2009).

Floch, H. G.

H. G. Floch and P. F. Belleville, J. Sol-Gel Sci. Technol. 2, 695 (1994).

Germain, C. V.

P. M. Pegon, C. V. Germain, Y. R. Rorato, P. F. Belleville, and E. Lavastre, Proc. SPIE 5250, 170 (2004).

Grosso, D.

D. Grosso and P. A. Sermon, Thin Solid Films 368, 116 (2000).

Guo, Y.

Y. Guo, X. Zu, X. Jiang, X. Yuan, S. Xu, H. Lv, and B. Wang, Optik 120, 437 (2009).

Hu, L.

H. Li, Y. Tang, and L. Hu, Acta Opt. Sin. (in Chinese) 29, 558 (2009).

H. Li, Y. Tang, and L. Hu, Chinese J. Lasers (in Chinese) 36, 472 (2009).

Jiang, X.

Y. Guo, X. Zu, X. Jiang, X. Yuan, S. Xu, H. Lv, and B. Wang, Optik 120, 437 (2009).

Kaneko, S.

H. Hayashi H. Suzuki, and S. Kaneko, J. Sol-Gel Sci. Technol. 12, 87 (1998).

Kozuka, H.

H. Kozuka, S. Takenaka, H. Tokita, and M. Okubayashi, Journal of the European Ceramic Society 24, 1585 (2004).

Lavastre, E.

P. M. Pegon, C. V. Germain, Y. R. Rorato, P. F. Belleville, and E. Lavastre, Proc. SPIE 5250, 170 (2004).

Li, H.

H. Li, Y. Tang, and L. Hu, Acta Opt. Sin. (in Chinese) 29, 558 (2009).

H. Li, Y. Tang, and L. Hu, Chinese J. Lasers (in Chinese) 36, 472 (2009).

Liang, L.

L. Liang, Y. Xu, D. Wu, and Y. Sun, Mater. Chemistry Phys. 114, 252 (2009).

Lv, H.

Y. Guo, X. Zu, X. Jiang, X. Yuan, S. Xu, H. Lv, and B. Wang, Optik 120, 437 (2009).

Mcinnes, H. A.

N. Bazin, J. E. Andrew, and H. A. Mcinnes, J. Sol-Gel Sci. Technol. 13, 757 (1998).

Ochs, C. J.

R. Carrion, F. Sittner, C. J. Ochs, S. Flege, and W. Ensinger, Thin Solid Films 517, 1967 (2009).

Okubayashi, M.

H. Kozuka, S. Takenaka, H. Tokita, and M. Okubayashi, Journal of the European Ceramic Society 24, 1585 (2004).

Pegon, P.

P. Belleville and P. Pegon, Proc. SPIE 3492, 244 (1999).

Pegon, P. M.

P. M. Pegon, C. V. Germain, Y. R. Rorato, P. F. Belleville, and E. Lavastre, Proc. SPIE 5250, 170 (2004).

Rorato, Y. R.

P. M. Pegon, C. V. Germain, Y. R. Rorato, P. F. Belleville, and E. Lavastre, Proc. SPIE 5250, 170 (2004).

Sermon, P. A.

D. Grosso and P. A. Sermon, Thin Solid Films 368, 116 (2000).

Shen, J.

G. Wang, J. Shen, Z. Xie, G. Wu, and Y. Xiao, Chinese J. Lasers (in Chinese) 33, 380 (2006).

Sittner, F.

R. Carrion, F. Sittner, C. J. Ochs, S. Flege, and W. Ensinger, Thin Solid Films 517, 1967 (2009).

Sun, Y.

L. Liang, Y. Xu, D. Wu, and Y. Sun, Mater. Chemistry Phys. 114, 252 (2009).

Suzuki, H. Hayashi H.

H. Hayashi H. Suzuki, and S. Kaneko, J. Sol-Gel Sci. Technol. 12, 87 (1998).

Takenaka, S.

H. Kozuka, S. Takenaka, H. Tokita, and M. Okubayashi, Journal of the European Ceramic Society 24, 1585 (2004).

Tang, Y.

H. Li, Y. Tang, and L. Hu, Chinese J. Lasers (in Chinese) 36, 472 (2009).

H. Li, Y. Tang, and L. Hu, Acta Opt. Sin. (in Chinese) 29, 558 (2009).

Thomas, I. M.

I. M. Thomas, Proc. SPIE 2288, 50 (1994).

I. M. Thomas, Appl. Opt. 31, 6145 (1992).

Tokita, H.

H. Kozuka, S. Takenaka, H. Tokita, and M. Okubayashi, Journal of the European Ceramic Society 24, 1585 (2004).

Wang, B.

Y. Guo, X. Zu, X. Jiang, X. Yuan, S. Xu, H. Lv, and B. Wang, Optik 120, 437 (2009).

Wang, G.

G. Wang, J. Shen, Z. Xie, G. Wu, and Y. Xiao, Chinese J. Lasers (in Chinese) 33, 380 (2006).

Wu, D.

L. Liang, Y. Xu, D. Wu, and Y. Sun, Mater. Chemistry Phys. 114, 252 (2009).

Wu, G.

G. Wang, J. Shen, Z. Xie, G. Wu, and Y. Xiao, Chinese J. Lasers (in Chinese) 33, 380 (2006).

Xiao, Y.

G. Wang, J. Shen, Z. Xie, G. Wu, and Y. Xiao, Chinese J. Lasers (in Chinese) 33, 380 (2006).

Xie, Z.

G. Wang, J. Shen, Z. Xie, G. Wu, and Y. Xiao, Chinese J. Lasers (in Chinese) 33, 380 (2006).

Xu, S.

Y. Guo, X. Zu, X. Jiang, X. Yuan, S. Xu, H. Lv, and B. Wang, Optik 120, 437 (2009).

Xu, Y.

L. Liang, Y. Xu, D. Wu, and Y. Sun, Mater. Chemistry Phys. 114, 252 (2009).

Yuan, X.

Y. Guo, X. Zu, X. Jiang, X. Yuan, S. Xu, H. Lv, and B. Wang, Optik 120, 437 (2009).

Zu, X.

Y. Guo, X. Zu, X. Jiang, X. Yuan, S. Xu, H. Lv, and B. Wang, Optik 120, 437 (2009).

Acta Opt. Sin. (in Chinese) (1)

H. Li, Y. Tang, and L. Hu, Acta Opt. Sin. (in Chinese) 29, 558 (2009).

Appl. Opt. (1)

Chinese J. Lasers (in Chinese) (2)

H. Li, Y. Tang, and L. Hu, Chinese J. Lasers (in Chinese) 36, 472 (2009).

G. Wang, J. Shen, Z. Xie, G. Wu, and Y. Xiao, Chinese J. Lasers (in Chinese) 33, 380 (2006).

J. Sol-Gel Sci. Technol. (3)

N. Bazin, J. E. Andrew, and H. A. Mcinnes, J. Sol-Gel Sci. Technol. 13, 757 (1998).

H. G. Floch and P. F. Belleville, J. Sol-Gel Sci. Technol. 2, 695 (1994).

H. Hayashi H. Suzuki, and S. Kaneko, J. Sol-Gel Sci. Technol. 12, 87 (1998).

Journal of the European Ceramic Society (1)

H. Kozuka, S. Takenaka, H. Tokita, and M. Okubayashi, Journal of the European Ceramic Society 24, 1585 (2004).

Mater. Chemistry Phys. (1)

L. Liang, Y. Xu, D. Wu, and Y. Sun, Mater. Chemistry Phys. 114, 252 (2009).

Optik (1)

Y. Guo, X. Zu, X. Jiang, X. Yuan, S. Xu, H. Lv, and B. Wang, Optik 120, 437 (2009).

Proc. SPIE (3)

P. M. Pegon, C. V. Germain, Y. R. Rorato, P. F. Belleville, and E. Lavastre, Proc. SPIE 5250, 170 (2004).

I. M. Thomas, Proc. SPIE 2288, 50 (1994).

P. Belleville and P. Pegon, Proc. SPIE 3492, 244 (1999).

Thin Solid Films (2)

R. Carrion, F. Sittner, C. J. Ochs, S. Flege, and W. Ensinger, Thin Solid Films 517, 1967 (2009).

D. Grosso and P. A. Sermon, Thin Solid Films 368, 116 (2000).

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