Abstract

A new transparent Tm3+-doped ZrF4-based nanocrystallized glass with the composition of 55ZrF4-20BaF2-18.8YF3-5AlF5-1.2TmF3 (mol%) (ZBYA) has been prepared by a conventional melting quenching technique and the subsequent heat treatment processes. The glass characteristic temperatures, the apparent activation energy, and the Avrami parameter for crystallization are estimated on the basis of different scanning calorimetry (DSC). The sizes of grown nanocrystals in the glass matrix appear to be 30-36.5 nm and it is studied as a function of the nucleation temperature, also the peak intensity of the nanocrystalline is studied as a function of the nucleation temperature from the X-ray diffraction (XRD) measurement. The microhardness measurement shows that the Vickers microhardness (Hv) values of the heat-treated glass samples are larger than that of the based glass about 17.26%-42.04%.

© 2006 Chinese Optics Letters

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  1. M. Poulain, J. Non-Cryst. Solids 184, 103 (1995).
  2. J.-L. Adam, J. Fluorine Chem. 107, 265 (2001).
  3. W. A. Pisarski, J. Pisarska, T. Goryczka, G. Dominiak-Dzik, and W. Ryba-Romanowski, J. Alloys and Compounds 398, 272 (2005).
  4. K. E. Lipinska-Kalita, F. Auzel, and P. Santa-Cruz, J. Non-Cryst. Solids 204, 188 (1996).
  5. H. Ebendorff-Heidepriem, I. Szabo, and Z. E. Rasztovits, Opt. Mater. 14, 127 (2000).
  6. M. Mortier, A. Monteville, G. Patriarche, G. Maze, and F. Auzel, Opt. Mater. 16, 255 (2001).
  7. F. Auzel, K. E. Lipinska-Kalita, and P. Santa-Cruz, Opt. Mater. 5, 75 (1996).
  8. P. Santa-Cruz, D. Morin, J. Dexpert-Ghys, A. Sadoc, and F. Auzel, J. Non-Cryst. Solids 190, 238 (1995).
  9. J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Non-Cryst. Solids 188, 285 (1995).
  10. J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Am. Ceram. Soc. 79, 2397 (1996).
  11. J. M. Jewel1, J. Jaganathan, and I. D. Aggarwal, J. Am. Ceram. Soc. 74, 788 (1991).
  12. H. S. Chen, J. Non-Cryst. Solids 27, 257 (1978).
  13. J. A. Augis and J. E. Bennett, J. Therm. Anal. 13, 283 (1978).

2005 (1)

W. A. Pisarski, J. Pisarska, T. Goryczka, G. Dominiak-Dzik, and W. Ryba-Romanowski, J. Alloys and Compounds 398, 272 (2005).

2001 (2)

J.-L. Adam, J. Fluorine Chem. 107, 265 (2001).

M. Mortier, A. Monteville, G. Patriarche, G. Maze, and F. Auzel, Opt. Mater. 16, 255 (2001).

2000 (1)

H. Ebendorff-Heidepriem, I. Szabo, and Z. E. Rasztovits, Opt. Mater. 14, 127 (2000).

1996 (3)

J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Am. Ceram. Soc. 79, 2397 (1996).

F. Auzel, K. E. Lipinska-Kalita, and P. Santa-Cruz, Opt. Mater. 5, 75 (1996).

K. E. Lipinska-Kalita, F. Auzel, and P. Santa-Cruz, J. Non-Cryst. Solids 204, 188 (1996).

1995 (3)

M. Poulain, J. Non-Cryst. Solids 184, 103 (1995).

P. Santa-Cruz, D. Morin, J. Dexpert-Ghys, A. Sadoc, and F. Auzel, J. Non-Cryst. Solids 190, 238 (1995).

J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Non-Cryst. Solids 188, 285 (1995).

1991 (1)

J. M. Jewel1, J. Jaganathan, and I. D. Aggarwal, J. Am. Ceram. Soc. 74, 788 (1991).

1978 (2)

H. S. Chen, J. Non-Cryst. Solids 27, 257 (1978).

J. A. Augis and J. E. Bennett, J. Therm. Anal. 13, 283 (1978).

Adam, J.-L.

J.-L. Adam, J. Fluorine Chem. 107, 265 (2001).

Aggarwal, I. D.

J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Am. Ceram. Soc. 79, 2397 (1996).

J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Non-Cryst. Solids 188, 285 (1995).

J. M. Jewel1, J. Jaganathan, and I. D. Aggarwal, J. Am. Ceram. Soc. 74, 788 (1991).

Augis, J. A.

J. A. Augis and J. E. Bennett, J. Therm. Anal. 13, 283 (1978).

Auzel, F.

M. Mortier, A. Monteville, G. Patriarche, G. Maze, and F. Auzel, Opt. Mater. 16, 255 (2001).

F. Auzel, K. E. Lipinska-Kalita, and P. Santa-Cruz, Opt. Mater. 5, 75 (1996).

K. E. Lipinska-Kalita, F. Auzel, and P. Santa-Cruz, J. Non-Cryst. Solids 204, 188 (1996).

P. Santa-Cruz, D. Morin, J. Dexpert-Ghys, A. Sadoc, and F. Auzel, J. Non-Cryst. Solids 190, 238 (1995).

Bennett, J. E.

J. A. Augis and J. E. Bennett, J. Therm. Anal. 13, 283 (1978).

Chen, H. S.

H. S. Chen, J. Non-Cryst. Solids 27, 257 (1978).

Dexpert-Ghys, J.

P. Santa-Cruz, D. Morin, J. Dexpert-Ghys, A. Sadoc, and F. Auzel, J. Non-Cryst. Solids 190, 238 (1995).

Dominiak-Dzik, G.

W. A. Pisarski, J. Pisarska, T. Goryczka, G. Dominiak-Dzik, and W. Ryba-Romanowski, J. Alloys and Compounds 398, 272 (2005).

Ebendorff-Heidepriem, H.

H. Ebendorff-Heidepriem, I. Szabo, and Z. E. Rasztovits, Opt. Mater. 14, 127 (2000).

Friebele, E. J.

J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Am. Ceram. Soc. 79, 2397 (1996).

J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Non-Cryst. Solids 188, 285 (1995).

Goryczka, T.

W. A. Pisarski, J. Pisarska, T. Goryczka, G. Dominiak-Dzik, and W. Ryba-Romanowski, J. Alloys and Compounds 398, 272 (2005).

Jaganathan, J.

J. M. Jewel1, J. Jaganathan, and I. D. Aggarwal, J. Am. Ceram. Soc. 74, 788 (1991).

Jewel1, J. M.

J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Am. Ceram. Soc. 79, 2397 (1996).

J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Non-Cryst. Solids 188, 285 (1995).

J. M. Jewel1, J. Jaganathan, and I. D. Aggarwal, J. Am. Ceram. Soc. 74, 788 (1991).

Lipinska-Kalita, K. E.

F. Auzel, K. E. Lipinska-Kalita, and P. Santa-Cruz, Opt. Mater. 5, 75 (1996).

K. E. Lipinska-Kalita, F. Auzel, and P. Santa-Cruz, J. Non-Cryst. Solids 204, 188 (1996).

Maze, G.

M. Mortier, A. Monteville, G. Patriarche, G. Maze, and F. Auzel, Opt. Mater. 16, 255 (2001).

Monteville, A.

M. Mortier, A. Monteville, G. Patriarche, G. Maze, and F. Auzel, Opt. Mater. 16, 255 (2001).

Morin, D.

P. Santa-Cruz, D. Morin, J. Dexpert-Ghys, A. Sadoc, and F. Auzel, J. Non-Cryst. Solids 190, 238 (1995).

Mortier, M.

M. Mortier, A. Monteville, G. Patriarche, G. Maze, and F. Auzel, Opt. Mater. 16, 255 (2001).

Patriarche, G.

M. Mortier, A. Monteville, G. Patriarche, G. Maze, and F. Auzel, Opt. Mater. 16, 255 (2001).

Pisarska, J.

W. A. Pisarski, J. Pisarska, T. Goryczka, G. Dominiak-Dzik, and W. Ryba-Romanowski, J. Alloys and Compounds 398, 272 (2005).

Pisarski, W. A.

W. A. Pisarski, J. Pisarska, T. Goryczka, G. Dominiak-Dzik, and W. Ryba-Romanowski, J. Alloys and Compounds 398, 272 (2005).

Poulain, M.

M. Poulain, J. Non-Cryst. Solids 184, 103 (1995).

Rasztovits, Z. E.

H. Ebendorff-Heidepriem, I. Szabo, and Z. E. Rasztovits, Opt. Mater. 14, 127 (2000).

Ryba-Romanowski, W.

W. A. Pisarski, J. Pisarska, T. Goryczka, G. Dominiak-Dzik, and W. Ryba-Romanowski, J. Alloys and Compounds 398, 272 (2005).

Sadoc, A.

P. Santa-Cruz, D. Morin, J. Dexpert-Ghys, A. Sadoc, and F. Auzel, J. Non-Cryst. Solids 190, 238 (1995).

Santa-Cruz, P.

F. Auzel, K. E. Lipinska-Kalita, and P. Santa-Cruz, Opt. Mater. 5, 75 (1996).

K. E. Lipinska-Kalita, F. Auzel, and P. Santa-Cruz, J. Non-Cryst. Solids 204, 188 (1996).

P. Santa-Cruz, D. Morin, J. Dexpert-Ghys, A. Sadoc, and F. Auzel, J. Non-Cryst. Solids 190, 238 (1995).

Szabo, I.

H. Ebendorff-Heidepriem, I. Szabo, and Z. E. Rasztovits, Opt. Mater. 14, 127 (2000).

J. Alloys and Compounds (1)

W. A. Pisarski, J. Pisarska, T. Goryczka, G. Dominiak-Dzik, and W. Ryba-Romanowski, J. Alloys and Compounds 398, 272 (2005).

J. Am. Ceram. Soc. (2)

J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Am. Ceram. Soc. 79, 2397 (1996).

J. M. Jewel1, J. Jaganathan, and I. D. Aggarwal, J. Am. Ceram. Soc. 74, 788 (1991).

J. Fluorine Chem. (1)

J.-L. Adam, J. Fluorine Chem. 107, 265 (2001).

J. Non-Cryst. Solids (5)

M. Poulain, J. Non-Cryst. Solids 184, 103 (1995).

P. Santa-Cruz, D. Morin, J. Dexpert-Ghys, A. Sadoc, and F. Auzel, J. Non-Cryst. Solids 190, 238 (1995).

J. M. Jewel1, E. J. Friebele, and I. D. Aggarwal, J. Non-Cryst. Solids 188, 285 (1995).

K. E. Lipinska-Kalita, F. Auzel, and P. Santa-Cruz, J. Non-Cryst. Solids 204, 188 (1996).

H. S. Chen, J. Non-Cryst. Solids 27, 257 (1978).

J. Therm. Anal. (1)

J. A. Augis and J. E. Bennett, J. Therm. Anal. 13, 283 (1978).

Opt. Mater. (3)

H. Ebendorff-Heidepriem, I. Szabo, and Z. E. Rasztovits, Opt. Mater. 14, 127 (2000).

M. Mortier, A. Monteville, G. Patriarche, G. Maze, and F. Auzel, Opt. Mater. 16, 255 (2001).

F. Auzel, K. E. Lipinska-Kalita, and P. Santa-Cruz, Opt. Mater. 5, 75 (1996).

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