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Optica Publishing Group
  • Applied Spectroscopy
  • Vol. 56,
  • Issue 7,
  • pp. 920-927
  • (2002)

Broadband Spectroelectrochemical Attenuated Total Reflectance Instrument for Molecular Adlayer Studies

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Abstract

The study of thin film molecular architectures is an increasingly important endeavor with respect to the development and characterization of materials ranging from liquid crystalline displays to receptor-based biosensors. Here we describe an apparatus capable of simultaneously acquiring broadband spectroscopic and electrochemical information on molecularly thin films deposited on a transparent electrode surface through a multiple internal reflection geometry. To demonstrate the capabilities of this system, the spectroelectrochemical behavior of a single, neutral copper phthalocyanine bilayer was evaluated.

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