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Optica Publishing Group
  • Applied Spectroscopy
  • Vol. 43,
  • Issue 7,
  • pp. 1240-1248
  • (1989)

Quantitative Measurements of Adsorbed Aminosilanes on Muscovite Mica Using Diffuse Reflectance Infrared Fourier Transform Spectroscopy

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Abstract

A method for quantitative analysis of 3-aminopropyltriethoxysilane (γ-APS) and N-(N-vinylbenzy1-2-aminoethyl)-3-aminopropyltrimethoxysilane hydrochloride (cationic vinylbenzyl silane, CVBS) on muscovite mica powder has been developed with the use of diffuse reflectance FT-IR spectroscopy. The adsorption isotherms determined by this method are reported. The results are compared with a previous study of the adsorption of aminosilanes by ESCA, and possible models of the adsorbed layer are discussed.

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