The enantiomer separation and the spectral simplification of overlapped resonances in a high-resolution <sup>1</sup>H NMR spectrum of a model compound have been successfully accomplished with the use of paramagnetic shift reagent. Both <sup>1</sup>H and <sup>13</sup>C NMR have been applied to determine the composition of a mixture containing optically active enantiomers of (+/-)-2,2-dimethyl-1-phenyl-1-propanol.

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