The fundamental molecular vibration frequencies of dimethylsilanediol were studied and assigned based upon data collected by infrared and Raman spectroscopy, and upon the literature of analogous compounds. Dimethylsilanediol and dimethylsilane-d<sub>2</sub>-diol were prepared by the hydrolysis of dimethoxydimethylsilane with water and deuterium oxide, respectively. The purity of dimethylsilanediol was verified by a gas chromatographic technique. This research found the SiOH deformations of dimethylsilanediol to absorb at 1175 cm<sup>−1</sup> and 1060 cm<sup>−1</sup>

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