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  • Applied Spectroscopy
  • Vol. 36,
  • Issue 3,
  • pp. 285-289
  • (1982)

Raman Spectroscopic Investigation of Isomeric and Mixed-Valence Heteropolyanions

Melody Starr Kasprzak, G. E. Leroi, and S. R. Crouch

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Abstract

Raman spectroscopy has been used to distinguish structural differences between α-12-heteropoly anions and β-12-heteropoly anions in solution. The results are consistent with the Keggin structure for the α-isomers and a modified Keggin structure for the β-isomers. Reduced 12-molybdophosphates and molybdovanadophosphates in solution have also been characterized by Raman spectroscopy; the results are consistent with a retention of the Keggin structure.

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