Micro-Raman spectroscopy has been utilized to examine the spectra of solid samples of α-UF<sub>5</sub>, β-UF<sub>5</sub>, UF<sub>6</sub>, three types of UO<sub>2</sub>F<sub>2</sub>, the powder residue from a static UF<sub>6</sub> release, and γ-UO<sub>3</sub>. The spectra are presented and compared to previous literature values, with new features indicated where appropriate. With the implied constraint of proper sample handling, micro-Raman spectroscopy is a useful technique for the ready identification of uranium fluorides, oxyfluorides, and oxides.
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